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PEROXIDE

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FTC Korea

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ALKENOX-P100

ALKENOX P-100

Summary

ALKENOX P-100 is a white fine powder which has peroxy group in the molecular. It is generally used for initiator of polymerization in the unsaturated polyester resin, vinyl chloride
mono-polymerization & Copol ymerization.

Formula

- Formula :

- Name : Bis-(4-tert-butylcyclohexyl)
Peroxy dicarbonate
- CAS No : 15520-11-3
- Molecular weight : 398.64

Pyhsical Properity

- Appearance : White fine power
- Purity : Min. 95%
- Molecular weight : 398.64
- Temperature at 10 hrs half life : 44℃
- Activation energy : 30.2kcal / mol
- Solubility : insoluble in water,
- Soluble in Ketones, Esters, Aromatic
Hydrocarbon

Chemical Prooerity

- Strong oxidation agent. - Active oxygen content : Min 3.8% - Heat decomposition properties Half life of ALKENOX P-100 at 0.2 mol/mol in benzene
Temp (℃)	Half life(hours)
40	17.4
44	10
50	4
60	1
92	1
- Flash point : Room temperature - Combustion properties (sample 10g) Burning time : 5 sec Flame length : 100㎝

Decomposition Compound

ALKENOX P-100 is easy to decompose by hea The Mechanism of decomposition.

Safety Test

- Ignition temp. : Room temp
- Auto lgnition temp : 360℃
- Combustion properties (sample 10g)
  Combustion time : 5 sec
  Length of flame : 100 sec
  Drop-hammer sensitivity : 30Cm
  Pressure test : Max.0.7mm

Package

- Inner package : Polyethylene bag
- Ourter package : Craft paper box

Application

-The initiator of unsaturated polyester resin
ALKENOX P-100 has low decomposing temp(44℃). It is suitable for pulltrusion mold, continuous laminating and large scale mold. Especially large scale moding, heating furnace is needed to get a high temperature. ALKENOX P-100 which has low decomposing temp is suitable for that cases. ALKENOX P-100 is also used with other curing agent such as BPO(Benzoxl peroxide), TBPB(t-butyl-perbenzoate) and other metal salt accelerators. In that case, we can expect a improved properties after curing.

- Polymerization initiator of VCM(Vinyl Chloride Monomer)
ALKENOX P-100 is used for polymerization of VCM which is the monomer of PVC at 40~70℃

- Polymerization initiator of other monomer
ALKENOX P-100 is used as initiator of homopolymer
- ization & copolymerization of acrylate, methacrylate

ane vinylidene floride monomer-

Storage and Handling

The test report of storage safety of ALKENOX P-100

Period of storage	Decrease rate of active oxygen
Period of storage	30℃	40℃
1 week	-	1.5%
2 weeks	1.3%	2.6%
3 weeks	-	4.6%
4 weeks	1.3%	-
5 weeks	-	7.4%
6 weeks	2%	13%
7 weeks	3%	-
11 weeks	4.3%	-
24 weeks	6.4%	-

- Storage
   ALKENOX P-100 is quite active peroxide. However handling it at room temperature is possible as it's storage stability at room temperature is a rather high so it is possible to handle at room temperature.   But it can be decompesed at above 25℃, so it must be stored under 20℃ and kept away from direct sunligiht

- First aid
   Skin contact cause a hazard like other peroxides, so appropriate protection is needed. During working, protective clothes and protective hand cream is needed.
---Eye Contact : Immediately flush eyes with plenty of water.
Get medical attention immddiatly

---Skin Contact : Immediately flush skin with   plenty of soap and water. Get medical attention immediately.

---Ingestion : Not to vomit. Get medical attention
- Toxicological information
   Oral rat : LD 50 : >5g/㎏

Appendix

- Solublity Data (wt% conc)

Solvents	-20℃	0℃	10℃	20℃	30℃
Methanol	-	1	-	-	2.3
Hentane	-	7.5	-	-	17.5
Shellsol T	-	2	-	4.04	-
Shellsol K	-	-	-	5	-
MEK	11	24.7	-	-	31.4
MIBK	-	17.5	-	-	31.3
Benzene	-	29.3	46.7	-	49.3
Tpluene	-	33	-	-	49
MeAc	-	11.5	-	-	22.2
FtAc	-	16	-	-	32
Dibuth Phthalate	-	9.2	-	11.8	14.1
CCI4	-	19	-	-	21.5
Ethylene	-	-	-	-	-
teichloride	11	24.5	-	33	-
Viryl	-	-	-	-	-
Chloride	15	25	-	-	-
MMA	-	19.8	-	25	-

- Curing Properties & Pot life of curing agent

Initiator	Criti Cal Temp (℃)	80℃				Pot Life (hrs)
Initiator	Criti Cal Temp (℃)	G.T (min	C.T (min	T.max (℃)	Hard ness	30℃	40℃
ALKENOXP-100	50	0.6	1.1	231	47	10	3
Kayanox		1.6	2.8	209	42	3	1
Laubox		3	4.1	204	44	35	8
Trigonox 38	65	4	11.3	173	42	9	3
BPO	70	5.9	7.3	203	44	50	14
t-butyl perhenzoate	70	3.7	5.2	222	48	27	8
Trigonox 29~75%	70	8.4	10.7	200	47	70	22
Kayacarhon BIC-75	70	16.9	26.2	193	45	40	18
Kayanox A-M	80	3.3	6.3	197	43	70	3

Initiator	Criti Cal Temp (℃)	100℃				Pot Life (hrs)
Initiator	Criti Cal Temp (℃)	G.T (min)	C.T (min)	T.max (℃)	Hard ness	30℃	40℃
ALKENOXP-100	50	-	-	-	-	10	3
Kayanox		0.2	0.6	226	43	3	1
Laubox		0.3	0.7	210	45	35	8
Trigonox 38	65	1.5	2.9	229	46	9	3
BPO	70	1	15	248	47	50	14
t-butyl perhenzoate	70	0.2	0.5	223	50	27	8
Trigonox 29~75%	70	1.6	2.3	222	48	70	22
Kayacarhon BIC-75	70	2.9	4.2	237	45	40	18
Kayanox A-M	80	0.8	0.8	226	4.	70	3

※ Test Condition : JISK 6901, use unsaturated
polyester resin lnitiator : 1phr

- The combination of ALKENOXP-100 & other initiator

t-butyl perhenzoate

Using amount(phr)		80℃ Curing				Pot life (hrs)
ALKENOX P-100	t-butyl perhenzoate	G.T (min)	C.T (min)	T.max (℃)	Hard ness	Pot life (hrs)
0	1	3.8	5.2	222	45	26
0.2	0.8	2	2.9	224	45	16
0.5	0.5	1	1.6	221	45	11
0.8	0.2	0.6	1.2	223	45	9
1	0	0.5	0.9	226	45	8

BPO

Using amount(phr)		80℃ Curing				Pot life (hrs)
ALKENOX P-100	t-butyl perhenzoate	G.T (min)	C.T (min)	T.max (℃)	Hard ness	Pot life (hrs)
0	1	5.9	7.3	220	45	4~5
0.2	0.8	2.4	3.3	222	45	27
0.5	0.5	1	1.7	225	45	13
0.8	0.2	0.6	1.2	223	45	9
1	0	0.5	0.5	226	45	8

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FTC Korea

Minisite Heart

Country / Year Established: South Korea /

Business type: Others

TRADE TOWER

DUNS

President: Ma Younghun

Address: 982 Yongso-ri, Yanggam-myun, Hwasung-si, Gyeonggi-do, Korea

Product Category: Dyestuffs,Other Chemicals

Company introduction: We were established in Sept. 1999, capitalized at USD450,000.00 with annual sales turnover USD5Million fiscal year 2007, we have been a specialty chemicals manufacturer (ISO9001 accredited manufacturer & trader) to produce paint catalysts of acid/blocked/tin/polymerization, anti-foaming de-aerating agents, leveling agents, anti-flooding & pigment dispersing agents, Rheology control agents, functional epoxy/polyester/acrylic resins, etc. for Coil coating, Industrial coating and Automotive painting applications.

For your reference, I would like to inform you that FTC is conducting branch corp. from 2004 in Shanghai China and also we want you to refer that we have supplied our paint catalyst & levelling agent matching for King Industries & BYK to Shanghai Chen Hua Paint Manufacturing Co. who is the largest local paint manufacturer in China, regularly together with other 4~5 Clients annual total about 60MTY, and several Paint manufacturing Corporations invested from Korea, such as Samhwa Paint Co., Ltd., Kumgang Chemical Corp.(KCC), Daehan Paint Industries(DPI), Dongshin Paint Co., Ltd. in annual total 200MTY. On the other hand, we have also supplied our paint catalyst & additives to Vietnamese Clients from last year, and are planning to positively promote World market especially in North America, Europe, China, India, Indonesia, etc. from the second half of this year.

At the height of "2nd wave era of Globalization" publicated from IMD Switzerland this year, we are seriously looking for new reliable megalopolitan sales agent or future Client to enable us meet custom made marketing throughout the World.

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